序號(hào) | 名稱/型號(hào)/規(guī)格 | 數(shù)量 | 單位 | 備注 |
一 | 標(biāo)準(zhǔn)配置 | |||
1 | 主機(jī) | |||
1.1 | TQ-9001三重四極桿質(zhì)譜儀 | 1 | 臺(tái) | 含ESI、APCI離子源,集成注射泵、切換閥,一體式差分渦輪分子泵400/300 L/s,前級(jí)機(jī)械泵40 m3/h |
1.2 | SPH1299 二元泵 | 1 | 臺(tái) | 二元超高壓液相泵組,壓力1300 bar,內(nèi)置在線真空脫氣機(jī) |
1.3 | Alias 自動(dòng)進(jìn)樣器 | 1 | 臺(tái) | 制冷型、標(biāo)配2個(gè)48位樣品瓶架 |
1.4 | T190柱溫箱 | 1 | 臺(tái) | |
1.5 | 溶劑柜 | 1 | 臺(tái) | |
1.6 | 廢液底座 | 1 | 臺(tái) | |
1.7 | SV40機(jī)械泵 | 1 | 臺(tái) | 內(nèi)含預(yù)裝泵油1瓶 |
2.1 | B&C ITECH Chemstation V1.0數(shù)據(jù)采集軟件 | 1 | 套 | |
2.2 | B&C ITECH Chemstation數(shù)據(jù)處理軟件 | 1 | 套 | |
2.3 | ||||
3 | 外設(shè)/附件 | |||
3.1 | 啟動(dòng)工具包: | 1 | 套 | 隨機(jī)工具盒1套; 軟件1個(gè); 軟件U盤1個(gè); ESI 調(diào)諧液1瓶; 注射泵連接套裝1套: 1ml 注射器、 魯爾接頭、PEEK管線、PEEK 接頭; 安裝搬運(yùn)工具1套; 真空連接套件: 波紋管1根,KF40 卡箍2個(gè),KF40 中心支架2個(gè) 備用密封圈1套: 離子源密封圈4個(gè) QJET前密封圈1個(gè) QJET后密封圈1個(gè) 反吹氣密封圈1個(gè); |
3.2 | 儀器說(shuō)明書 | 1 | 份 | |
3.3 | 產(chǎn)品合格證、保修卡 | 1 | 套 | |
3.4 | ||||
選配品 | ||||
1.1 | 電腦 | 1 | 臺(tái) | |
1.2 | 打印機(jī) | 1 | 臺(tái) | |
2 | ||||
2.1 | UPS穩(wěn)壓電源 | 1 | 臺(tái) | |
2.2 | 氮?dú)獍l(fā)生器 | 1 | 臺(tái) | |
2.3 | ||||
4 | 備品/耗材 | |||
4.1 | 色譜柱 | 1 | 根 | |
4.2 | 樣品瓶 | 1 | 套 | |
4.3 | 樣品瓶蓋 | 1 | 套 |
Instrument Specification-Mass spectrometer (Triple Quadruple) | |
Mass range(m/z) | 5-2000 amu |
Scan speed | >10,000 amu/sec |
Mass Resolution | Unit Resolution FWHM,0.6-0.8 amu |
Mass stability | ± 0.1Da in 24 hours |
Sensitivity MRM mode | ESI+, Reserpine 1 pg on column, MRM609/195,S/N > 200,000 |
Repeatability | ESI+, Tacrolimus 5pg on column with 10 injections, Peak area RSD < 1.5%, Retention time RSD<0.25 |
Scan types | Full scan MS and selected ion for both Q1 and Q3, product ion scan, precursor ion scan, neutral loss or gain scan, Multiple reaction monitoring (MRM) |
Dynamic range | 6 orders of magnitude |
Ionization source | Ion Source housing with ESI Probe or APCI probe (max temp: 750ºC) ESI flow rate range: 5 μL/min to 3 mL/min APCI flow rate range: 200 µL/min to 3 mL/min |
Software | B&C ITECH Chemstation V1.0 |
Instrument Specification-Liquid Chromatograph (UHPLC) | |
Flow rate range | 0.001 - 2.00 ml/min, 0.001 ml/min increments |
Pressure range | 0-1300 bar |
Flow precision | ≤ 0.075 % RSD or 0.005 min SD, whichever is greater, H2O in a flow range of 0.200 - 2.000 mL/min |
Flow accuracy | ± 1% or ± 10 μL/min, whichever is greater, H2O in a flow range of 0.200 - 2.000 mL/min |
Gradient composition range | 0 - 99% (A in B) |
Gradient composition accuracy | ± 0.5 % absolute from 5 - 95%, H2O in a flow range of 0.200 - 2.000 mL/min |
Gradient composition precision | ≤ 0.15% or 0.01 min SD, whichever is greater, H2O in a flow range of 0.200 - 2.000 mL/min |
Injection modes | Full loop, partial loopfill and µL pickup mode |
Injection volume | Programmable from 0 uL-100 uL,1 µL increments |
Reproducibility | RSD £ 0.3% for full loop injections |
RSD £ 0.5% for partial loopfill injections, injection volumes > 5 µL at constant pressure RSD £ 1.0% for µL pickup injections, injection volumes > 5 µL | |
Carry-over | < 0.05% with programmable needle wash |
Viscosity range | 0.1 - 5 cP |
Sample tray cooling | Built-in Peltier cooling Range: 4°C to Ambient - 3°C Temp: air temperature in sample compartment: 4°C ± 2°C (at temperature sensor) (Temperature at relative humidity of 80% and ambient temperature of 25°C) |
Needle wash | Inside and outside needle wash with drying. Wash can be programmed between injections and between vials/wells. |
Sample capacity | Microtiter plates: 2 Vials: 2x 48 (1.5 mL) – optional Microtiter plates according to SBS standards. 96-well high and low and 384-well. |
Column Oven Temperature control mode | air circulation with heating module |
Temperature range | ambient+5°C - 60°C, with 1°C increments |
Temperature stability | Better than 0.1 °C |
Column capacity | Maximum 2 column, Length150 mm |